Grignard Synthesis of Benzoic Acid Lab Activity (ScholAR)

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ScholAR Grignard Synthesis of Benzoic Acid Lab Activity

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Aligned with AP Chemistry Lab #22

When a solution of an alkyl halide in an anhydrous solvent and an anoxic environment is allowed to stand over metallic magnesium, a vigorous reaction occurs that results in the formation of the Grignard reagent. Once the Grignard reagent is prepared it can be used to prepare the target compound, in this case a carboxylic acid. This experiment can be completed in 90 minutes and comes with enough materials for 15 setups. The Pyrex Micro-Organic Chemistry set or Combo-Still is required, available separately.
Chemical Contents:
Activated Carbon
Bromobenzene
Hydrochloric Acid, 6 M Solution
Iodine Crystals
Magnesium Metal Turnings
Tetrahydrofuran
Additional Materials Required:
Pyrex Micro Organic Chemistry Set or Combo-Still
Dry Ice, 50 g

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